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FCAL-9118-Front

Fluke Calibration 9118A Thermocouple Calibration Furnace

sku Product SKU:  FCAL-9118A

Seven key features set the 9118A apart from other high-temperature calibration furnaces:

1. WIDE TEMPERATURE RANGE SPANNING MOST HIGH-TEMPERATURE APPLICATIONS

Standards and guidelines such as AMS 2750 and EURAMET cg-8 require that a thermocouple be calibrated over the full temperature range in which it is used. The 9118A temperature range of 300 °C to 1200 °C covers most high-temperature applications.

2. FLEXIBLE CONFIGURATION FOR CALIBRATING A WIDE RANGE OF THERMOCOUPLE TYPES

The 9118A furnace can be operated with or without an isothermal block, which increases calibration workload that can be performed with a single furnace:

  • Tube furnace configuration (without isothermal block): Base-metal thermocouples are often sheathed in formable materials such as braided fiberglass or PTFE. During calibration, they are bundled around a reference thermometer, held together with fiberglass cord or tape, and inserted into a tube furnace.
  • Isothermal block configuration: Metal- or ceramic-sheathed thermocouples are generally constructed with noble-metal thermoelements and therefore have higher calibration accuracy requirements. The isothermal block, which accommodates up to four 6.35 millimeter probes, improves heat transfer and temperature stability. This better equalizes the temperature between the reference probe and the UUT, which lowers measurement uncertainty compared to calibration without a block.

The furnace configuration can be quickly changed by selecting the calibration parameters stored in the controller for the desired configuration and inserting or removing the alumina ceramic isothermal block.

3. BEST-IN-CLASS TEMPERATURE STABILITY AND UNIFORMITY FOR CALIBRATION ACCURACY

Axial and radial uniformity, as well as constant temperature stability over time, are key factors that contribute to accurate thermocouple calibrations.

To minimize axial temperature gradients, three actively controlled heater zones compensate for temperature differentials between the central zone and the front and rear zones. Type-S thermocouples, which are less susceptible to drift than other types, are used for zone control and cutout. Axial temperature uniformity when using the isothermal block is ± 0.2 °C over a 60 mm (2.4 in) zone from full immersion at 1200 °C.

Radial (hole-to-hole) uniformity is ± 0.25 °C at 1200 °C when using the isothermal block, and ± 0.5 °C over a 14 mm (0.6 in) diameter at the center of the furnace tube without a block. 

When using the isothermal block, temperature stability is ± 0.1 °C or better over the full temperature range of the furnace.

 No other calibration furnace in its class comes close to this level of performance for both modes of operation. 

4. AUTOMATED SETPOINT CONTROL FOR IMPROVED LAB PRODUCTIVITY

A proprietary programmable controller, available in nine languages (English, Chinese, French, German, Japanese, Korean, Portuguese, Spanish, and Russian), enables technicians to automate setpoint temperature control for up to eight setpoint temperatures, the temperature ramp rate, and the time duration the furnace controls at each setpoint.

Automation and data collection can be further enhanced when the Fluke 1586A Super-DAQ is connected to the 9118A furnace through the RS-232 interface. The Super-DAQ can be programmed to control the furnace's setpoint temperatures and collect data for all sensors under test once the furnace has stabilized to within parameters defined by the user. After data has been collected at the first programmed temperature, the Super-DAQ will advance the furnace to the remaining programmed temperatures, collecting data at each setpoint. Once the test has been configured and started, the technician can walk away to work on other activities. 

5. NON-METALLIC BLOCK HELPS MINIMIZE THERMOCOUPLE CONTAMINATION

Calibration furnaces with metallic blocks can contaminate thermocouples, causing their accuracy to drift over time. To minimize the risk of contamination, the furnace well and isothermal block of the 9118A are constructed of non-metallic, ceramic alumina. This eliminates the need to protect the thermocouples under test with costly ceramic sleeving—reducing cost of ownership.

6. DEEP IMMERSION DEPTH TO SUPPORT MOST THERMOCOUPLE CALIBRATIONS

Industry standards such as AMS2750 recommend calibrating thermocouples at their normal working depth of insertion. The 9118A immersion depth is 365 mm (14.4 in) when using the isothermal block and 350 mm (13.8 in) to the central point of the furnace without a block. This immersion depth is adequate for most of thermocouple calibrations. The 40 mm x 700 mm (1.6 in x 27.6 in) open-ended furnace tube can also be useful when calibrating multi-junction thermocouples or when sample testing spools of thermocouple wire.

 7. DYNAMIC HEATER CONTROL AND CUTOUTS FOR RELIABILITY AND SAFETY

The 9118A controls the heater power level below 100% to prevent the heater elements from overheating—improving heater reliability and lifetime. Redundant over-temperature cutouts are built into the 9118A to ensure safe operation of the furnace. These include over-temperature, chassis thermostat, fan fault, control thermocouple fault, and user programmable cutouts.

 

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Custom Temperature Calibration Baths

sku Product SKU:  FCL-Custom Temperatures Calibration Baths

Fluke Calibration temperature baths provide optimal temperature environments for “secondary” or “comparison” temperature calibrations. They offer unsurpassed stability and uniformity, a large working volume, and flexibility for performing thermometer calibration on calibrating a variety of temperature sensors. However, if your needs aren’t met by our standard sizes and temperature ranges, then we can build a custom bath that is as reliable and as fine a calibration instrument as any standard bath we manufacture.

Some of the examples of the custom baths we have built include significant bath tank changes (taller, wider or deeper), change in the temperature range, different height or particular shape, faster heat and cool rates. We have built baths that require windows or custom dimensions to accommodate test fixtures. We can do all of this and more. No other manufacturer supplies custom baths to their customers, but we do.

Our engineers and designers know more about temperature calibration baths than anyone else. You’ll find our baths throughout the best national and international temperature calibration labs. It does not matter what type of calibration application you have – oceanography, missile optics, infrared, sensor manufacturing, semiconductor, renewable energy, LIG manufacturing, or down-hole tools. We have probably already built baths to do the job.

 

 

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Calibration Bath Fluids

sku Product SKU:  FCL-Calibration Bath Fluids

Fluke Calibration carries a full line of bath fluids covering temperature ranges from –100°C to 550°C.

Finally, there’s a convenient source for small quantities of bath fluids for any temperature range. Why pay for more than you need?

Viscosity, volatility and other properties that change with temperature affect the performance of fluids in controlled baths and circulators. Fluke Calibration has tested and used each of the fluids we sell. Over the ranges recommended in the following table, each fluid remains at a low enough viscosity to be adequately pumped or stirred. Whether your application is industrial or critical lab calibration work, Hart fluids give you top performance and stability.

For temperature ranges too high for oils, we have a bath salt with a viscosity in the molten state similar to the viscosity of water. For your convenience, it is shipped in a granular form, making it easy to fill your bath.

Between its melting point of 150°C and 550°C, this salt has the highest temperature stability and uniformity available in a bath fluid. It does not smoke like oils or give off dust like “sand" or fluidized alumina baths. Check with your bath manufacturer before using this salt to make sure your equipment is compatible. Fluke Calibration offers three standard bath models and custom-designed units for use with this salt.

Fluid specifications 
It’s important to understand a few specifications before selecting a bath fluid. We’ve seen bath fluids advertised with a temperature range that spans from the freezing point to the flash point or beyond.

For example, type 710 silicone oil has a freezing point of –22°C, but freezing point has nothing to do with the point at which the oil becomes so thick it cannot be properly stirred. Type 710 oil should really only be used down to about 80°C. It’s a viscosity issue, not a freezing-point issue. Usable range is the question. Suitability for calibration work is the specification that counts.

The usable viscosity range is determined by your bath’s stirring or pumping design. Fluke Calibration baths can be operated using fluids with up to 50 centistokes viscosity. This gives you additional usable range in the lower temperature levels of the fluid.

Some baths advertised as calibration baths require fluids with 10 centistokes or less viscosity to operate properly. The usable ranges in our table on the previous page assume the use of a Fluke bath.

In addition to range and viscosity issues, there are a number of other issues to consider when choosing a bath fluid. The other considerations are:

  • Thermal characteristics
  • Lifetime
  • Change in characteristics due to temperature cycling
  • Absorption of water from the air
  • Vaporization—fumes and fume hood requirements
  • Expansion due to heat
  • Contamination—mixing oils or introducing contamination with unclean probes
  • Conductivity properties
  • Effects of using fluids outside of their range—fire, explosion, polymerization
  • Effects of altitude on boiling point

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    Liquid Trap

    sku Product SKU:  FCL-Liquid Trap

    The 7000-102 Liquid Trap can be used with most any pneumatic test or calibration system where liquid contamination may be present in the device under test. Although the preferred procedure is to insure the device under test is free of both liquid and particulate contamination prior to calibration, the 7000-102 provides a degree of insurance to protect the calibration instrument.

    The 7000-102 can be used with any calibrator, including the Model 7010 and complete line of Series 7215 Digital Pressure Controllers. It can assist with minimizing the possibility of contamination of the unique Ruska quartz sensor found in these instruments along with the control valves and solenoid valves, all of which are designed for pneumatic operation and can be damaged when exposed to liquids.  

    The 7000-102 is also compatible with Druck’s line of pressure controllers including the DPI 515 and DPI 520 Digital Pressure Calibrators.

    Further, the 7000-102 can be used with virtually any test or calibration system where the pressure does not exceed 3000 psi. 

    A convenient drain valve allows periodic removal of accumulated liquids. Due to the pressure range, the level inside the Trap cannot be observed. Therefore it is recommended that the drain valve be opened on a frequent basis or prior to each test. A fitting is provided on the drain valve to allow connection to tubing that can run to a container for disposal.

    The 7000-102 Liquid Trap is provided with a bench mount stand with two mounting holes for a sturdy installation.

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    Fluke Calibration 155X Stik Thermometer

    sku Product SKU:  FCAL-155X Stik

    Finally, a digital substitute for your mercury-in-glass thermometers! Accurate and repeatable to ± 0.05 °C over its full range, the 1551A/1552A “Stik Thermometer is the new “gold standard" of industrial temperature calibration. Whether working outdoors in environments where potentially explosive gases may be present or on the floor of a processing plant, the intrinsically-safe, battery operated, portable reference thermometer is designed to go where you work.
     

    Features at a glance

    • Accuracy of ± 0.05 °C (± 0.09 °F) over full range
    • Intrinsically safe (ATEX and IECEx compliant)
    • Two models to choose from (-50 °C to 160 °C or -80 °C to 300 °C)
    • User-configurable temperature Trend/Stability indicator
    • Display temperature in °C or °F
    • Optional data logging to internal memory
    • 300-hour battery life
    • Percent battery-life and low-battery indicator
    • NVLAP-accredited, NIST-traceable calibration included

    Thermometer probe and digital readout combined into one unit

    The stainless steel probe and digital readout are fixed together and calibrated as a system. The accuracy specification is easy to understand since it includes all uncertainty components, including drift, for up to one year1. The large backlit LCD display rotates 90° degrees making it easy to read from any angle. A user-configurable stability/trend indicator lets you know when your temperature is stable enough to record an accurate measurement. A user-settable auto-off function extends typical battery life to three hundred hours. A low-battery indicator and stop-measure function prevent erroneous measurements from being made due to low battery life. A simple three-point calibration function allows you to easily and accurately calibrate the “Stik" Thermometer. Data logging to internal memory of up to 10,000 time-stamped measurements is optionally available.

    Why calibrate process temperature sensors?

    Because temperature greatly effects the accuracy of a volumetric measurement, process manufacturers of chemical, pharmaceutical, food or petroleum products require accurate temperature measurements—especially for processes where quality or custody transfer are regulated by government agencies. Since all temperature sensors are subject to drift with time, regular calibration or verification against a reliable reference thermometer is required. Finding a reference thermometer that is accurate, repeatable and robust, however, can be challenging.

    What’s wrong with my reference thermometer?

    Industrial reference thermometers available on the market today, such as mercury-in-glass thermometers (or “ASTM thermometers") and portable electronic thermometers are useful, but both come with inherent problems. Although accurate and repeatable, mercury thermometers are fragile. The risk of a mercury spill poses potential hazards to the environment and to the health of personnel. Many of the United States and European Union countries have already banned their use in industrial applications. Some organizations have replaced their mercury thermometers with more durable portable electronic thermometers, only to discover that the RTD probes lack the repeatability and dependability required of a legitimate reference thermometer.

    The best alternative to mercury thermometers

    The Fluke “Stik" Thermometer is accurate, stable and durable, making it the best alternative to mercury thermometers and existing electronic thermometers. The thin-film RTD sensor incorporates the same characteristics of other premium reference thermometers designed by Hart Scientific, but it is more robust and less susceptible to drift. Accuracy and repeatability, however, are not sacrificed for improved durability.

    Using a glass-stem mercury- or spirit-filled thermometer at different immersion depths, or at significantly different ambient temperatures from which it was calibrated, may require the application of emergent-stem corrections that can be tedious but necessary to calculate an accurate measurement. This isn’t required with the “Stik" Thermometer. The sensor of the 1551A Ex requires a minimum immersion depth of only seven centimeters (2.8 inches), with no appreciable effect on the measured temperature due to heat loss through stem conduction. Some digital thermometers can become less accurate when used outside a narrow range of ambient temperatures. This isn’t the case for the “Stik" Thermometer. Your measurement remains accurate in ambient temperatures from -10 degrees to 50 degrees celsius (14 degrees to 122 degrees fahrenheit). With a superior probe design combined with electronic functions that assist accurate measurement, the “Stik" Thermometer surpasses the capabilities of other digital thermometers and is the perfect substitute for your mercury thermometers. 1In order to minimize sensor drift, the probe should always be protected from mechanical shock.

    Five reasons to replace mercury thermometers

    1. Since the “Stik" Thermometer does not contain mercury, it is not subject to government-imposed bans. Government agencies worldwide have either banned or are seeking to ban the use and transportation of industrial mercury thermometers—this seems to be a growing trend.
    2. The stainless steel probe sheath of the “Stik" Thermometer is far more robust than the glass stem of a mercury thermometer and better suited for industrial environments. And since the “Stik" thermometer does not contain mercury, the risk of an accidental mercury spill is eliminated.
    3. When considering cost of ownership, a digital thermometer is less expensive than a mercury thermometer. With a mercury thermometer, you either invest in equipment or you hire out to clean up after a mercury spill.
    4. Mercury thermometers cannot be adjusted after calibration. The actual temperature must be calculated by applying corrections to the measured temperature. This costs time and is susceptible to calculation error. A digital thermometer does the math for you—the displayed temperature accurately represents the actual measured temperature.
    5. Emergent-stem corrections may also be required if the mercury thermometer is not used under the same conditions under which it was calibrated. A digital thermometer doesn’t require that you match calibration conditions to achieve an accurate measurement. You’re only required to meet the minimum immersion requirements—which is only seven centimeters (2.8 inches) in the case of the 1551A Ex.

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